Early Soil Nitrate Trends after Wheat in 2022

Small grain harvest is well underway across the region, and soil testing is progressing quickly. Crop yields have varied from below average to exceeding expectations across the region and often in the same area. Planting date, summer temperatures, and rainfall (too little or too much) were major factors this year.

The major factors influencing the amount of residual soil nitrate-N after crops are:

1.     Nitrogen fertilizer rate: too high or too low
2.     Crop yield achieved: much lower or higher than expected
3.     Nitrogen losses: denitrification and leaching after too much rainfall
4.     Nitrogen mineralization from organic matter: cool or warm growing season

Seasonal weather is a large driving factor in the amount of nitrate-N in the soil profile. This changes from field to field and year to year. Early spring weather conditions were very wet across much of the region. In June and July, some areas continued to receive adequate to excess rainfall. Meanwhile, other areas received very little rain in the late growing season.

AGVISE has tested over 10,000 soil samples from wheat fields across the region. The table below indicates the percentage of soil samples in each soil nitrate-nitrogen category in several areas of Manitoba, Minnesota, North Dakota, and South Dakota. The data should give you a general idea of how variable residual soil nitrate is from field to field in each region. With such variable crop yields, there is quite a bit of variability in residual nitrate following wheat in the region. In drought-affected areas of Minnesota, North Dakota, and South Dakota, over 10 to 20% of soil samples have more than 60 lb/acre nitrate-N (0-24 inch soil profile) remaining after wheat.

What about Prevented Planting or unseeded acres?

For Prevented Planting or unseeded acres, the factors above plus some additional factors will affect the amount of residual nitrate-nitrogen:

1.     How long was water standing on the field?
2.     Was weed growth controlled, early or late?
3.     Was tillage used? How many times? How deep?
4.     Was a cover crop planted? What amount of growth was achieved?

When submitting soil samples from fields that were not planted, please choose “Fallow” or “Cover Crop” as the previous crop. This will allow us to send additional information on soil nitrate trends for unseeded and cover crop fields once we get enough data.

As the fall soil testing season continues, we will keep you updated. If you have any questions, please call our experienced agronomic staff. We hope you have a safe harvest and soil testing season.

 

Prevented Planting Acres? What to do for 2023

This article originally appeared in the AGVISE Laboratories Fall 2022 Newsletter

Good crop prices encouraged late planting beyond crop insurance deadlines, but additional June rainfall kept some producers from planting all their acres, leaving some unplanted fields or unplanted parts of fields. There are many questions about soil testing on these unplanted fields: When should you start soil sampling? What kind of residual soil nitrate-nitrogen amounts can you expect? The extremely wet soil conditions may have caused considerable soil nitrogen losses to leaching or denitrification. Through summer, warmer and drier weather added nitrogen through mineralization of soil organic matter. In addition, cover crops and any weedy growth will acquire nitrogen from soil. The amount of soil nitrate-nitrogen remaining for next year will depend on soil type, environment, and management factors, which vary from field to field and zone to zone.

Management Factors
• What was the crop grown in the previous year?
• What was the nitrogen fertilizer rate and application timing? Was it applied last fall?
• Did you do any summer tillage? More tillage promotes nitrogen mineralization.
• How was your weed control? Did the weeds get large and acquire substantial nitrogen?
• Did you plant a cover crop? Did the cover crop get incorporated later?

Environmental Factors
• Did excessive rainfall cause nitrate leaching on well-drained soils?
• Did excessive rainfall cause denitrification on poorly drained soils?
• Were summer temperatures warm? Warm temperatures promote N mineralization.

Soil testing on these unplanted fields can begin as soon as good quality soil samples can be collected after mid-August. There is no reliable way to guess how much residual soil nitrate may be present in these unplanted fields or unplanted parts of fields. Soil testing is the only accurate way to learn how much residual soil nitrate remains in the soil profile. To obtain the best information for nitrogen management, we recommend splitting fields into management zones for soil testing. The unplanted field areas can vary considerably from the rest of the field, which will skew the field-average soil test result and resulting nitrogen fertilizer rate.

Soil Sampling for Nitrogen in a Delayed Spring

Spring planting is clipping along in some parts of the region, while other parts are still waiting to hit the field, as excessive rainfall and cold temperatures have delayed spring field work and planting. Who would have thought last fall that this is what spring 2022 would look like, after the worst region-wide drought in 30 years? Mother Nature always reminds us to stay prepared for anything.

A delayed spring start means that every day in the field is important. AGVISE delivers next-day turnaround on processing soil samples. The soil samples are analyzed and reported the next business day after arrival at the laboratory. Soil test results are posted to our online AGVISOR portal for quick and easy access. If you need any soil sampling supplies for spring, please let us know and we will send them to you right away.

So, what is the best strategy for spring soil testing and assessing soil nitrogen losses after the rain? The compressed fertilizer and planting window might not leave enough time to adjust preplant fertilizer rates, especially if the field is just barely dry enough to plant. If soil nitrogen losses have occurred following spring rains, a spring soil test collected now will be helpful to create a split-applied nitrogen plan or to direct a supplemental nitrogen application later. In the AGVISE Spring 2022 Newsletter, we answered some questions on split-applied nitrogen application strategies, so please take a look at those options for applying nitrogen during the growing season.

Short-season crops develop quickly, so additional nitrogen should be applied in the upcoming weeks. A soil sample collected before or shortly after planting will provide the best assessment of preplant soil nitrogen supply and losses. Do not wait too long to collect the soil sample because, as we move into June, plant nitrogen uptake and nitrogen mineralization from soil organic matter will make the soil nitrogen result more difficult to decipher. To maximize yield in small grains, apply all topdress nitrogen before jointing (5-leaf stage). Any nitrogen applied after jointing will mostly go to grain protein. In canola, apply nitrogen during the rosette stage, before the 6-leaf stage.

Long-season crops like corn offer more flexibility and time for in-season soil sampling and nitrogen application. Rapid nitrogen uptake in corn does not begin until after the V6 growth stage. The Pre-sidedress Soil Nitrate Test (PSNT) can help you decide the appropriate sidedress nitrogen rate. For more details, take a look at the PSNT article link for instructions on collecting and submitting PSNT soil samples. The PSNT requires a 0-12 inch depth soil sample taken when corn plants are 6 to 12 inches tall (at the whorl), usually in late May or early June. Late-planted corn may not reach that height before mid-June, but PSNT soil samples should still be collected during the first two weeks of June. If spring rainfall was above normal, Iowa State University guidelines provide additional PSNT interpretation criteria for excessive rainfall, manured soils, and corn after alfalfa.

If you have any questions on the best strategies for spring soil sampling and in-season nitrogen application options, please call our technical support team and we will be happy to answer any questions you may have.

Zone Soil Sampling and Variable Rate Fertilization: Optimizing profits

This article originally appeared in the AGVISE Laboratories Winter 2022 Newsletter

Farmers, like all business owners, are profit maximizers: things are good when revenue exceeds cost. Things are even better when the difference between revenue and costs is substantial. The math behind increasing profit is simple: reduce costs, increase revenue. But, the difficult part is finding and implementing strategies on the farm to do this. Why not start with fertilizer, which is typically the largest annual input cost on the farm?

Your fields are variable. You know the hilltops have lower crop yields than the mid-slopes, and you know exactly how far the saline spots creep into the more productive part of the field. So why use the same rate of fertilizer in the unproductive areas as you would in the productive areas? Optimize your fertilizer inputs by reducing rates in low-yielding areas and reallocate those fertilizer dollars to the productive ground.

The North Field Zone Map

Figure 1. North Field zone map, created using ADMS from GK Technology.

How does one actually do this? Creating zone maps for your fields, soil sampling and testing based on productivity zones, and variable rate (VRT) fertilizer application is the place to start. Applying VRT fertilizer allows you to apply fertilizer where it is needed and not waste fertilizer dollars where it is not. Let me show you an example from my family’s farm in western North Dakota.

I farm with my dad and brother in southwest North Dakota. This past fall, I created zone maps for each of our fields, with help from GK Technology and their ADMS program. The final maps are based on historical satellite imagery. I will show you one of our fields, the North Field, and take a deep dive on nitrogen fertilizer optimization using zone soil sampling and VRT fertilization in the dryland “out west” country.

The North Field (Figure 1) is variable. That is expected on a 120-acre field with many hills and ravines (Table 1). For discussion, we will use residual soil nitrate-nitrogen results and make a nitrogen fertilizer plan using urea for hard red spring wheat (HRSW) in 2022. You can see the soil nitrogen data, crop yield goals, and final nitrogen rates in Table 2.

 

The first place to optimize fertilizer inputs is setting realistic crop yield goals for each zone. Spring wheat yield goals range from 65 bushel/ acre in the best zone (zone 1) to 30 bushel/acre on the hilltops (zone 5). Adjusting the nitrogen rate for the proper crop yield goal ensures that the high-producing zones are not limited by lack of nitrogen (increased fertilizer cost, increased revenue) and the low-producing zones are not overfertilized (decreased fertilizer cost, same revenue). With a responsible crop yield goal on the low-producing zones, the crop still receives the amount of nitrogen it requires, and excess nitrogen is not lost to nitrate leaching (wasted input cost). As a result, the excess nitrogen fertilizer is reallocated to high-producing zones, resulting in more crop yield with the same total fertilizer budget, and increased revenue.

The nitrogen fertilizer scenarios in Tables 3 and 4 break down the projected revenues and expenses, demonstrating the benefits of zone soil sampling and VRT fertilization. For the North Field on my farm, the projected profit increase was $3,725 for the field or $31.05 per acre. It is tough to argue with a dollar amount like that! Prices will vary, of course, for fertilizer and precision ag services in your geography. Do the math for yourself and see how zone soil sampling and VRT fertilization can maximize profits for you.

2021 Drought: High residual soil nitrate-nitrogen across the region

This article originally appeared in the AGVISE Laboratories Winter 2022 Newsletter

The 2021 drought rivals the 1988 drought, and it covered much of the northern Great Plains and Canadian Prairies. From previous experience with droughts, we expected that residual soil nitrate-N following crops would be higher than normal, caused by the drought and reduced crop yields. The first wheat fields that were soil tested in August and September confirmed our expectation that residual soil nitrate-N was already trending much higher than normal.

The 2021 AGVISE soil test summary data highlights how exceptional the 2021 drought was. The median amount of soil nitrate-N across the region was markedly higher following wheat and corn. Over 20% of wheat fields had more than 100 lb/acre nitrate-N (0-24 inch) remaining, and another 40% of wheat fields had a sizable 40 to 80 lb/acre nitrate-N (0-24 inch) left over. For any given farm, the great variability in residual soil nitrate-N makes choosing one single nitrogen fertilizer rates impossible, and soil testing is the only way to decide that right rate for each field.

Through zone soil sampling, we were also able to identify that residual soil nitrate-N varied considerably within a field. This makes sense because we know that some areas of the field produced a fair yield, leaving behind less soil nitrate, while other areas produced very poorly and left behind much more soil nitrate. These differences across the landscape are driven by soil texture, soil organic matter, and stored soil water as well as specific problems like soil salinity or low soil pH (aluminum toxicity). Although the regional residual soil nitrate-N trends were higher overall, it is truly through zone soil sampling that we can begin to make sense of the field variability that drives crop productivity and the right fertilizer rate for next year.

For fields that have not been soil tested yet, there is still time to collect soil samples in winter (see winter soil sampling article). Nobody wants to experience another drought, but this kind of weather reminds us how important soil nitrate testing is every year for producers in the Great Plains. Each year, AGVISE summarizes soil test data for soil nutrients and properties in our major trade region of the United States and Canada. For more soil test summary data and other crops, please take a look at our soil test summaries online.

 

 

Banding Phosphorus and Potassium: Stretch your fertilizer dollars further

This article originally appeared in the AGVISE Laboratories Winter 2022 Newsletter

Broadcast or band? For phosphorus and potassium, these are big fertilizer questions. In recent months, high fertilizer prices have prompted farmers and agronomists to consider other strategies to reduce fertilizer costs without jeopardizing crop yield. Among the most common and effective options is placing fertilizer in a tight band below the soil surface, also known as a subsurface band.

Subsurface banding helps improve fertilizer recovery and efficiency. It ensures that fertilizer is placed in the plant root zone, facilitating direct uptake of crop nutrients. It also minimizes potential fixation reactions (aka tie-up) that reduce soil nutrient availability, allowing more phosphorus or potassium to remain available in soil for plant uptake. You ultimately get more bang for your buck on each pound of fertilizer applied. In addition, placing fertilizer below the soil surface protects fertilizer from

Idealized crop response to phosphorus as affected by fertilizer placement and soil test level (figure from J. Prod. Agric. 1:70-79).

soil erosion and runoff losses via wind and water. This is important for fall-applied phosphorus and potassium because spring snowmelt runoff and wind erosion can move fertilizer lying on the soil surface from neighbor to neighbor and watersheds beyond.

When we discuss banding phosphorus and potassium, it also comes along with the question, “How far can I cut fertilizer rates?” It is important to recognize that the improved efficiency of banding over broadcast is a function of soil test levels (figure) and proximity to the seed row. If you have high soil test levels (>15 ppm Olsen P), then the expected crop yield response to fertilizer, whether broadcast or banded, is lower. Banding fertilizer still helps with the fertilizer recovery, but the expected crop yield increase is often similar to broadcast. However, if you have low soil test levels, then the expected crop yield response is much greater with banding.

Where does seed row proximity fit in? The greatest efficiency comes with in-furrow or near-seed placement (e.g. 2×2 band), allowing effective fertilizer rates of one-half to two-thirds their broadcast equivalent. The near-seed placement also provides the starter effect, which enhances early plant growth and development in cool, wet soils of the upper Midwest and northern Great Plains. Of course, you must watch seed safety with any seed-placed fertilizer in the furrow.

For deep-band or mid-row band placement, the benefits over broadcast begin to disappear. These are still great placement options for anhydrous ammonia or urea, but the greater distance between the seed row and fertilizer band does not provide the same efficiency for immobile soil nutrients like phosphorus and potassium. This will surprise some people hoping that strip-till with deep-banded phosphorus and potassium or a one-pass air seeder with mid-row banders might be their answer to reducing fertilizer costs. For these “far-from-seed” banding options, reduced fertilizer rates are not suggested, and some in-furrow or near-seed banded fertilizer should still be applied for the current crop.

 

Fall-applied Nitrogen Fertilizer: A Couple Simple Rules

The beginning to mid-October is when soil temperatures across the northern Great Plains and Canadian Prairies typically drop below 50 °F (10 °C). This is the soil temperature threshold that we wait to reach before applying fall-applied nitrogen fertilizer. It is important to wait until soil temperatures are cold enough (<50 °F) to help reduce the risk of soil nitrogen loss. Once nitrogen fertilizer is applied, soil microbes begin converting ammonium-nitrogen (NH4+) to nitrate-nitrogen (NO3), a process called nitrification. In the nitrate form, nitrogen is vulnerable to loss through nitrate leaching or denitrification. The colder soil temperatures slow microbial activity, thus keeping more nitrogen in the safer ammonium-nitrogen form. This applies to any ammoniacal nitrogen fertilizer source, which includes anhydrous ammonia, urea, and ammonium sulfate.

Map courtesy of the North Dakota Agricultural Weather Network (NDAWN).
You can find an updated average bare soil temperature map here

The 50 °F soil temperature rule of thumb is particularly important for soils prone to nitrogen loss: well-drained, coarse-textured soils are prone to nitrate leaching and poorly-drained, fine-textured soils are prone to denitrification. If such soils receive excess precipitation or become saturated (waterlogged) through fall or spring, soil nitrate can be lost through leaching or denitrification. In general, it might be better to apply nitrogen fertilizer on such soils in spring. But, if you must apply nitrogen fertilizer in the fall, make sure you wait until soil temperatures are cold enough to keep it in the ammonium-nitrogen form for a longer period of time to reduce potential soil nitrogen losses.

For fall-applied nitrogen, subsurface banding or incorporation is also important to prevent ammonia volatilization, another potential nitrogen loss mechanism. Fall precipitation (rain or snow) is too sporadic and unreliable to be considered an effective incorporation “strategy” for fall-applied nitrogen. Fall-applied urea should be banded below the soil surface (3 inches or deeper) or incorporated with tillage (at least 3-4 inches) to ensure complete coverage. Shallow fertilizer bands or shallow incorporation with vertical tillage does not provide enough soil coverage to prevent ammonia volatilization.

Fall-applied anhydrous ammonia should be banded 5 to 6 inches deep. Ensure that anhydrous ammonia trenches are sealing properly to prevent gaseous ammonia losses from the trench. In addition, the nitrification inhibitor nitrapyrin (brand name N-Serve) can be added to anhydrous ammonia to delay nitrification, offering additional insurance to keep nitrogen in the safer ammonium-nitrogen form for longer. However, please note that its efficacy decreases with warmer soil temperatures, so it is no replacement for cool soil temperatures (<50 °F).

In conclusion, fall-applied nitrogen is a great way to allocate time and labor resources, leaving one less thing to do in the spring. But, you must be smart and consider fertilizer source, timing, and placement options to make sure that the nitrogen applied in fall will still be there next spring.

How much residual soil nitrate is left after the 2021 corn crop?

It’s probably more than you think.

So far, the residual soil nitrate-nitrogen trend following corn is much higher than average across the upper Midwest and northern Great Plains. This follows the same trend set by the 2021 wheat crop. For many growers in the region, the hot and dry growing season has resulted in high residual soil nitrate-N carryover where corn yield was lower than average. An update on average residual soil nitrate-N after grain and silage corn, broken into zip code areas, can be found below (Table 1). This data highlights the importance of soil sampling for nitrate-N, even after high N-requirement crops you may not think of leaving much residual soil nitrate-N behind.

Bar graph showing median residual nitrate-N in lb/acre for fields sampled after grain corn as of Oct. 11, 2021. Results include fields tested in MN, ND, SD, and MB. Fields tested thus far are on pace to set a record for amount of nitrate-N left after corn.

The early soil nitrate-N trend data gives us a snapshot of the soil samples that AGVISE has analyzed so far. The average soil test data is not a replacement for actual soil test results on your fields or your clients’ fields. There is considerable variability within a single zip code area, with some corn fields having less than 20 lb/acre nitrate-N and many other fields that are much higher. Take a look at eastern South Dakota, the Sioux Falls and Watertown areas have over 49% of soil samples with more than 100 lb/acre nitrate-N (0-24 inch soil depth). Considering sky-high nitrogen fertilizer prices (and still rising), it makes sense to soil test for nitrate-N and credit it toward next year’s crop nitrogen budget.

Agronomic considerations for soybean in 2022

One crop that will not benefit from extra residual soil nitrate-N after corn is soybean. Soybean can create its own nitrogen thanks to a symbiotic relationship with nitrogen-fixing bacteria. The nitrogen fixation process takes energy, however, and if there is already ample plant-available nitrate in the soil, soybean will delay nodulation and take advantage of the free nitrate. Delayed nodulation may ultimately lead to soybean yield loss.

High residual soil nitrate-N can also increase soybean iron deficiency chlorosis (IDC) severity.  Soybean IDC is a challenge for growers in the upper Midwest, northern Great Plains, and Canadian Prairies, especially on soils with high carbonate and salinity. If soil nitrate-N is also high, research has shown it can make soybean IDC even worse and result in lower soybean yield. If you plan to grow soybean on fields with high residual soil nitrate-N, seriously consider IDC-tolerant soybean varieties or consider planting them on fields with lower residual soil nitrate-N.

Should a corn-corn rotation be considered after a drought year and high soil nitrate?

Planting a second corn crop would allow a producer to capture this “free” nitrate-N in the soil profile. However, planting corn on corn has many challenges from soil moisture to insect pressures (e.g. corn rootworm). The 2021 corn crop started the growing season with a full profile of water (due to excessive moisture in 2019 and adequate moisture in 2020) and ended with enough to push the corn crop through harvest. Going into the 2022 growing season, plant available water will be considerably less than the beginning of 2021. If the drought continues into 2022, remember that corn requires more moisture than soybean, so planting corn on corn means putting a higher water-requiring crop on ground that had less water to start with (versus corn following soybeans). Less available moisture, combined with other agronomic pressures, may mean less than expected yield for a corn-on-corn rotation.

Table 1. Residual nitrate trends as of Oct. 11, 2021 from more than 2,500 soil samples taken after corn. Regions with less than 60 soil samples are not included in the table.

Soil Sample Before Tillage: Consistent sample depth matters!

The fall harvest season is a busy time of year. Farmers need to finish harvest, apply fertilizer, and complete any tillage operations before the long winter sets in. Another field operation that needs to be completed within this flurry of activity is soil sampling, and sampling timing is crucial to getting quality and consistent soil cores.

Do your best to soil sample fields before any tillage pass. Tillage makes collecting soil cores with consistent depths very difficult, which can affect test results. Soil test results are only as reliable as the soil samples that were collected from the field. If a sample is submitted as a 0 to 6-inch sample and is only really the top 0 to 4-inch of the soil, soil test values are inflated compared to actual 0 to 6-inch results. The opposite happens if a core is actually deeper than the 0 to 6-inch depth: soil test values are diluted if the sample that was submitted is deeper. The table below shows an example of how test levels of non-mobile nutrients like P, K, and Zn decrease as soil core length increases.

Why tillage affects sampling depth consistency and core quality

Tillage breaks apart soil and introduces air, essentially “fluffing” the soil. Sampling after the soil has been “fluffed” means the sampler has to guess what actually represents a 6-inch soil depth for that field. What was a 0 to 6-inch core in the soil probe before tillage might actually take up 8 inches in the soil probe now, given the soil profile is now “fluffy” after tillage. Over time the soil will settle, but when does that happen? How fast does that happen? When will 0 to 6 inches of tilled soil in the soil probe actually represent a 0 to 6-inch depth again? No one can accurately answer these questions.

Beyond the soil being “fluffy” after tillage, tillage loosens soil aggregates, makes clods, and generally dries the soil. This means loose soil may fall out of the probe or the probe pushes around the clods at the surface and does not get a true 0 to 6-inch sample. This might mean a core that’s collected and sent to the laboratory might actually be a 2 to 8-inch depth core, or a 2 to 6-inch depth core.

A tip for sampling after tillage

If you have to sample after tillage, sample in the wheel track. The tire compresses the soil and allows you to get a better opportunity at a true 0 to 6-soil core depth.

Getting consistent soil core depths is crucial. Sampling before tillage is the best thing you can do to ensure quality cores with consistent depths. Sampling after tillage can result in lower test levels for non-mobile nutrients like P, K, and Zn. Please call either AGVISE laboratory and ask for one of our technical support staff if you have any questions about sampling after a field has been tilled. 

Corn Stalk Nitrate Test

To help evaluate nitrogen management in corn, you may want to try the corn stalk nitrate test as a post-mortem tool. The corn stalk nitrate test is a late-season or end-of-season plant analysis on mature corn stalks. Iowa State University developed the corn stalk sampling protocol and interpretation. If corn did not have sufficient nitrogen, the corn stalk nitrate level will be low. If corn had excess nitrogen, the corn stalk nitrate level will be high.

The corn stalk nitrate test can be useful in cropping systems with manure or corn-after-alfalfa, where a significant portion of the crop nitrogen budget comes from nitrogen mineralization. It is also helpful in more humid climates, where the residual soil nitrate-nitrogen test is not utilized. For corn silage production, it is easy to collect corn stalk samples on the go during silage harvest, making it a quick and useful tool.

Since the corn stalk nitrate test is a post-mortem tool with the goal to provide information for future years, it is not recommended in years with abnormal precipitation. In drought years, potential crop productivity is reduced, so the plant nitrogen requirement is lower than normal. In high precipitation years, soil nitrogen losses will reduce the available nitrogen supply. As a result, the corn stalk nitrate level can be very high in drought years or very low in wet years. Such results say more about environmental conditions, not the adequacy of the nitrogen fertilizer program.

When to sample

  • Early: One-quarter milk line (R5 growth stage) on majority of corn kernels. Nitrate concentration may be high if collected early.
  • Optimum: One to three weeks after physiological maturity (black layer, R6 growth stage) on 80% of corn kernels.
  • Late: Up to harvest. Nitrate concentration may be low if rainfall has leached nitrate from plant material.

How to sample

  • Measure 6 inches from the ground, cut the next 8 inches of corn stalk (the 6-14 inch stalk section measured from plant base). Remove outside leaf sheath.
  • Collect 12 to 15 corn stalks.
  • Place corn stalks in a ventilated plant tissue bag. Do not use plastic or zipped bag.
  • Do not collect diseased or damaged corn stalks.

Table 1. Corn Stalk Nitrate Test Interpretation

Nitrate-N (NO3-N), ppm Interpretation Comment
<250 Low Nitrogen supply was likely deficient and limited corn grain yield
250-2000 Sufficient
>2000 High Nitrogen supply exceeded plant requirement

for corn stalk nitrate test article